TRANSPORTABLE HIGH SENSITIVITY SMALL SAMPLE RADIOMETRIC CALORIMETER*

Year
1998
Author(s)
T. E. Sampson - Los Alamos National Laboratory
R. Biddle - Los Alamos National Laboratory,
J. R. Wetzel - Los Alamos National Laboratory
H.R. Dye - Los Alamos National Laboratory
Abstract
A new small-sample, high-sensitivity transportable radiometric calorimeter, which can be operated in different modes, contains an electrical calibration method, and can be used to develop secondary standards, will be described in this presentation. The data taken from preliminary tests will be presented to indicate the precision and accuracy of the instrument. The calorimeter and temperature-controlled bath, at present, require only a 30-in. by 20-in. tabletop area. The calorimeter is operated from a laptop computer system using a unique measurement module capable of monitoring all necessary calorimeter signals. The calorimeter can be operated in the normal calorimeter equilibration mode, as a comparison instrument, using twin chambers and an external electrical calibration method. The sample chamber is 0.75 in. (1.9 cm) in diameter by 2.5 in. (6.35 cm) long. This size will accommodate most 238Pu heat standards manufactured in the past. The power range runs from 0.001 W to